Methods for the Generation and Characterization of …

Cryogenic Milling. Polystyrene culture test tubes (Fisherbrand, 1119382) were first cut into 2–4 mm pieces. Approximately 5 g total mass of cut pieces were then milled using a stainless-steel ball mill (Retsch CryoMill, Haan, Germany) in a 50 ml chamber with a single 25 mm diameter stainless steel ball such that the total milling volume (including the ball) …

Reactivity Enhancement and Fabrication of Al-MoO

To prepare the Al-MoO 3 composite powder for kinetic spraying, an arrested reactive milling (ARM) method was performed using the Planetary Mill Pulverisette 5 (FRITSCH, Germany). The powders were milled in stainless-steel jars with SUS 316 balls (9.525Φ). Milling speed was fixed to 150 rpm. The ball and powder were added at a …

Speeding Up Your Organic Synthesis with Ball Mills

a milling material: agate, 20 min, 800rpm ≙ 13.3 Hz. b 20 min at 20 °C with maximal power input. c 60 in at 80 °C. d 30 min at 80 °C, maximal power input = 300 W.. The effective transfer of energy from the power socket into a product of interest has been proven for a number of examples. When different ball mills are compared with respect to …

Efficient degradation of trimethoprim with ball-milled …

The optimized MoS 2 /BC-0.5–4 with mass ratio of MoS 2 to BC of 0.5 and ball milling time of 4 h exhibited the highest degradation efficiency of TC at the present of PMS which significantly surpassed pristine BC and MoS 2. The results of XRD, FT-IR and Raman tests implied the composite was synthesized successfully.